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Title: :  Synthesis and Structural Characterization of Ni2+ , Cu2+, Pd2+ and Pt2+ complexes of 2,2'-(butane-2,3- diylidene)bis(hydrazine-1-carbothioamide)
PaperId: :  11895
Published in:   International Journal Of Advance Research And Innovative Ideas In Education
Publisher:   IJARIIE
e-ISSN:   2395-4396
Volume/Issue:    Volume 6 Issue 3 2020
DUI:    16.0415/IJARIIE-11895
Licence: :   IJARIIE is licensed under a Creative Commons Attribution-ShareAlike 4.0 International License.

Author NameAuthor Institute
Mohamad M.E. ShakdofaInorganic Chemistry Department, National Research Centre (ID 60014618), 33 El-Bohouth St., P.O. 12622, Dokki, Giza, Egypt
Fathy A. El-SaiedChemistry Department, Faculty of Science, El-Menoufia University, Shebin El-Kom, Egypt
Mayada S. AliChemistry Department, Faculty of Science, Kuwait University, P.O. Box 5969, Safat 13060, Kuwait
Reham M.W. FariedChemistry Department, Faculty of Science, El-Menoufia University, Shebin El-Kom, Egypt

Abstract

Inorganic Chemistry
Thiosemicarbazone, metal complexes, Electronic spectrum, NMR, IR
Ni2+, Cu2+, Pd2+ and Pt2+ complexes of of 2,2'-(butane-2,3-diylidene)bis(hydrazine-1-carbothioamide) (H2L) were prepared and fully characterized. The characterization of the prepared compounds were carried out analytical-ly and spectrally using elemental and thermal analyses, FTIR, 1H NMR, 13C NMR, mass and electronic absorp-tion spectra as well as magnetic and molar conductance measurements.The analytical data revesled that the complexes formed in 1:1 molar ratio and all complexes are non-electrolyte. The spectral data showed that the of 2,2'-(butane-2,3-diylidene)bis(hydrazine-1-carbothioamide) (H2L) behaved as a dibasic tetradentate chelator bonded with the metal ions via thiol sulphur atoms and azomethine nitrogen atoms adopting a square planar geometry for Ni2+ , Pd2+ and Pt2+ complexes, while Cu2+ complex adopts a distorted octahedral geometry structure. The thermal analysis showed that the ligand was stable up to 191C while Ni2+, Pd2+ and Pt2+ com-plexes were stable up to temperatures range from 235-320 C and decomposed in one step leading to the for-mation metal oxide or metal with carbon.

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IJARIIE Mohamad M.E. Shakdofa, Fathy A. El-Saied, Mayada S. Ali, and Reham M.W. Faried. "Synthesis and Structural Characterization of Ni2+ , Cu2+, Pd2+ and Pt2+ complexes of 2,2'-(butane-2,3- diylidene)bis(hydrazine-1-carbothioamide)" International Journal Of Advance Research And Innovative Ideas In Education Volume 6 Issue 3 2020 Page 13-23
MLA Mohamad M.E. Shakdofa, Fathy A. El-Saied, Mayada S. Ali, and Reham M.W. Faried. "Synthesis and Structural Characterization of Ni2+ , Cu2+, Pd2+ and Pt2+ complexes of 2,2'-(butane-2,3- diylidene)bis(hydrazine-1-carbothioamide)." International Journal Of Advance Research And Innovative Ideas In Education 6.3(2020) : 13-23.
APA Mohamad M.E. Shakdofa, Fathy A. El-Saied, Mayada S. Ali, & Reham M.W. Faried. (2020). Synthesis and Structural Characterization of Ni2+ , Cu2+, Pd2+ and Pt2+ complexes of 2,2'-(butane-2,3- diylidene)bis(hydrazine-1-carbothioamide). International Journal Of Advance Research And Innovative Ideas In Education, 6(3), 13-23.
Chicago Mohamad M.E. Shakdofa, Fathy A. El-Saied, Mayada S. Ali, and Reham M.W. Faried. "Synthesis and Structural Characterization of Ni2+ , Cu2+, Pd2+ and Pt2+ complexes of 2,2'-(butane-2,3- diylidene)bis(hydrazine-1-carbothioamide)." International Journal Of Advance Research And Innovative Ideas In Education 6, no. 3 (2020) : 13-23.
Oxford Mohamad M.E. Shakdofa, Fathy A. El-Saied, Mayada S. Ali, and Reham M.W. Faried. 'Synthesis and Structural Characterization of Ni2+ , Cu2+, Pd2+ and Pt2+ complexes of 2,2'-(butane-2,3- diylidene)bis(hydrazine-1-carbothioamide)', International Journal Of Advance Research And Innovative Ideas In Education, vol. 6, no. 3, 2020, p. 13-23. Available from IJARIIE, https://ijariie.com/AdminUploadPdf/Synthesis_and_Structural_Characterization_of_ijariie11895.pdf (Accessed : 02 April 2021).
Harvard Mohamad M.E. Shakdofa, Fathy A. El-Saied, Mayada S. Ali, and Reham M.W. Faried. (2020) 'Synthesis and Structural Characterization of Ni2+ , Cu2+, Pd2+ and Pt2+ complexes of 2,2'-(butane-2,3- diylidene)bis(hydrazine-1-carbothioamide)', International Journal Of Advance Research And Innovative Ideas In Education, 6(3), pp. 13-23IJARIIE [Online]. Available at: https://ijariie.com/AdminUploadPdf/Synthesis_and_Structural_Characterization_of_ijariie11895.pdf (Accessed : 02 April 2021)
IEEE Mohamad M.E. Shakdofa, Fathy A. El-Saied, Mayada S. Ali, and Reham M.W. Faried, "Synthesis and Structural Characterization of Ni2+ , Cu2+, Pd2+ and Pt2+ complexes of 2,2'-(butane-2,3- diylidene)bis(hydrazine-1-carbothioamide)," International Journal Of Advance Research And Innovative Ideas In Education, vol. 6, no. 3, pp. 13-23, May-Jun 2020. [Online]. Available: https://ijariie.com/AdminUploadPdf/Synthesis_and_Structural_Characterization_of_ijariie11895.pdf [Accessed : 02 April 2021].
Turabian Mohamad M.E. Shakdofa, Fathy A. El-Saied, Mayada S. Ali, and Reham M.W. Faried. "Synthesis and Structural Characterization of Ni2+ , Cu2+, Pd2+ and Pt2+ complexes of 2,2'-(butane-2,3- diylidene)bis(hydrazine-1-carbothioamide)." International Journal Of Advance Research And Innovative Ideas In Education [Online]. volume 6 number 3 (02 April 2021).
Vancouver Mohamad M.E. Shakdofa, Fathy A. El-Saied, Mayada S. Ali, and Reham M.W. Faried. Synthesis and Structural Characterization of Ni2+ , Cu2+, Pd2+ and Pt2+ complexes of 2,2'-(butane-2,3- diylidene)bis(hydrazine-1-carbothioamide). International Journal Of Advance Research And Innovative Ideas In Education [Internet]. 2020 [Cited : 02 April 2021]; 6(3) : 13-23. Available from: https://ijariie.com/AdminUploadPdf/Synthesis_and_Structural_Characterization_of_ijariie11895.pdf
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