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Title: :  STRUCTURAL AND THERMAL STUDIES OF MAGNESIUM TARTRATE CRYSTALS GROWN BY GEL TECHNIQUE
PaperId: :  25149
Published in:   International Journal Of Advance Research And Innovative Ideas In Education
Publisher:   IJARIIE
e-ISSN:   2395-4396
Volume/Issue:    Volume 10 Issue 5 2024
DUI:    16.0415/IJARIIE-25149
Licence: :   IJARIIE is licensed under a Creative Commons Attribution-ShareAlike 4.0 International License.

Author NameAuthor Institute
Nehaben H. TandelVeer Narmad South Gujarat University,Surat,Gujarat. India
Dr. I. B. PatelVeer Narmad South Gujarat University, Surat, Gujarat, India

Abstract

Material Science,Physics
Crystal Growth, XRD, TGA, FTIR, UV-Vis, SEM, EDAX, Gel growth
Tartrate crystals have wide applications. So, their growth procedure and their characteristics are very significant for industrial development. For the applications, the grown crystals have to be characterized and evaluated for their properties and behaviour. Single crystals of magnesium tartrate tetrahydrate were grown by single diffusion silica gel technique at ambient temperature. The obtained crystals were opaque having dimensions of 3 X 2 X 2 mm3. The powder XRD analysis showed these crystals to have orthorhombic crystal system. The lattice parameters are found to be; a = 9.1820 Å, b= 11.2062 Å and c = 7.9529 Å. FTIR spectral analysis confirmed the presence of water of crystallization and various related groups and bonds. The presence of expected elements in crystals was confirmed by carrying out EDAX spectrum analysis. UV-Vis-NIR spectral study reveals these crystals to be transparent and suitable for second harmonic generations. The obtained band gap energy value in the present study is found to be 4.776 eV. The scanned images show these crystals to be grown by layer deposition. Thermogravimetric analysis (TGA) confirms the presence of water molecules in the lattices and reveals the decomposition behavior of the crystals in the temperature range of 30-800 oC. Experimental data of TGA are used to generate the chemical formula for grown MT crystals. MT crystals are found to possess a chemical formula: MgC4H4O6.4H2O with a molecular weight of 244.403. The thermal stability of the crystals was found to be 39 oC. By using the standard Broido relation, the activation energy and various kinetic parameters such as change in entropy, change in enthalpy and Gibbs free energy for all the crystals were obtained and studied.

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IJARIIE Nehaben H. Tandel, and Dr. I. B. Patel. "STRUCTURAL AND THERMAL STUDIES OF MAGNESIUM TARTRATE CRYSTALS GROWN BY GEL TECHNIQUE" International Journal Of Advance Research And Innovative Ideas In Education Volume 10 Issue 5 2024 Page 1731-1739
MLA Nehaben H. Tandel, and Dr. I. B. Patel. "STRUCTURAL AND THERMAL STUDIES OF MAGNESIUM TARTRATE CRYSTALS GROWN BY GEL TECHNIQUE." International Journal Of Advance Research And Innovative Ideas In Education 10.5(2024) : 1731-1739.
APA Nehaben H. Tandel, & Dr. I. B. Patel. (2024). STRUCTURAL AND THERMAL STUDIES OF MAGNESIUM TARTRATE CRYSTALS GROWN BY GEL TECHNIQUE. International Journal Of Advance Research And Innovative Ideas In Education, 10(5), 1731-1739.
Chicago Nehaben H. Tandel, and Dr. I. B. Patel. "STRUCTURAL AND THERMAL STUDIES OF MAGNESIUM TARTRATE CRYSTALS GROWN BY GEL TECHNIQUE." International Journal Of Advance Research And Innovative Ideas In Education 10, no. 5 (2024) : 1731-1739.
Oxford Nehaben H. Tandel, and Dr. I. B. Patel. 'STRUCTURAL AND THERMAL STUDIES OF MAGNESIUM TARTRATE CRYSTALS GROWN BY GEL TECHNIQUE', International Journal Of Advance Research And Innovative Ideas In Education, vol. 10, no. 5, 2024, p. 1731-1739. Available from IJARIIE, https://ijariie.com/AdminUploadPdf/STRUCTURAL_AND_THERMAL_STUDIES_OF_MAGNESIUM_TARTRATE_CRYSTALS_GROWN_BY_GEL_TECHNIQUE_ijariie25149.pdf (Accessed : ).
Harvard Nehaben H. Tandel, and Dr. I. B. Patel. (2024) 'STRUCTURAL AND THERMAL STUDIES OF MAGNESIUM TARTRATE CRYSTALS GROWN BY GEL TECHNIQUE', International Journal Of Advance Research And Innovative Ideas In Education, 10(5), pp. 1731-1739IJARIIE [Online]. Available at: https://ijariie.com/AdminUploadPdf/STRUCTURAL_AND_THERMAL_STUDIES_OF_MAGNESIUM_TARTRATE_CRYSTALS_GROWN_BY_GEL_TECHNIQUE_ijariie25149.pdf (Accessed : )
IEEE Nehaben H. Tandel, and Dr. I. B. Patel, "STRUCTURAL AND THERMAL STUDIES OF MAGNESIUM TARTRATE CRYSTALS GROWN BY GEL TECHNIQUE," International Journal Of Advance Research And Innovative Ideas In Education, vol. 10, no. 5, pp. 1731-1739, Sep-Oct 2024. [Online]. Available: https://ijariie.com/AdminUploadPdf/STRUCTURAL_AND_THERMAL_STUDIES_OF_MAGNESIUM_TARTRATE_CRYSTALS_GROWN_BY_GEL_TECHNIQUE_ijariie25149.pdf [Accessed : ].
Turabian Nehaben H. Tandel, and Dr. I. B. Patel. "STRUCTURAL AND THERMAL STUDIES OF MAGNESIUM TARTRATE CRYSTALS GROWN BY GEL TECHNIQUE." International Journal Of Advance Research And Innovative Ideas In Education [Online]. volume 10 number 5 ().
Vancouver Nehaben H. Tandel, and Dr. I. B. Patel. STRUCTURAL AND THERMAL STUDIES OF MAGNESIUM TARTRATE CRYSTALS GROWN BY GEL TECHNIQUE. International Journal Of Advance Research And Innovative Ideas In Education [Internet]. 2024 [Cited : ]; 10(5) : 1731-1739. Available from: https://ijariie.com/AdminUploadPdf/STRUCTURAL_AND_THERMAL_STUDIES_OF_MAGNESIUM_TARTRATE_CRYSTALS_GROWN_BY_GEL_TECHNIQUE_ijariie25149.pdf
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